HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 13019381, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 2,3-Dihydroxypropyl 4-(n-hexadecylamino)benzoate | HCID 13019380 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 13019381 | HCID 13019381 | — |
Reaction Steps
A solution of 15.0 g of 2,3-dihydroxypropyl 4-(n-hexadecylamino)benzoate in 700 ml of carbon tetrachloride is stirred under reflux and is treated with anhydrous hydrogen chloride. The mixture is allowed to cool and is filtered to yield 2,3-dihydroxypropyl 4-(n-hexadecylamino)benzoate hydrochloride as a white solid, mp 126°-130° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04146546 |
| Source dataset | uspto-grants-1979_03 |
| ORD ID | ord-0175864eb99d4bc49da141ceb9e3f9a4 |
| Source note | uspto-grants-1979_03 |