HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 21326939, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 2,3-Dihydroxypropyl 4-(n-hexadecylamino)benzoate | HCID 13019380 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 21326939 | HCID 21326939 | — |
Reaction Steps
A solution of 6.53 g of 2,3-dihydroxypropyl 4-(n-hexadecylamino)benzoate in 100 ml of chloroform is stirred under reflux while 9.0 ml of acetic anhydride is added and for 6 hours thereafter. The solution is extracted with 2% aqueous sodium carbonate solution and water, dried, and evaporated to yield 2,3-diacetoxypropyl N-acetyl-4-(n-hexadecylamino)benzoate as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04146546 |
| Source dataset | uspto-grants-1979_03 |
| ORD ID | ord-200e7fb921354d8eb6a0d7ca8dd09507 |
| Source note | uspto-grants-1979_03 |