HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4-Hexadecylaminobenzoyl chloride hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 70506019 | HCID 70506019 | — |
| Product | 4-Hexadecylaminobenzoyl chloride hydrochloride | HCID 13255322 | — |
Reaction Steps
A mixture of 1.00 g of 4-(n-hexadecylamino)benzoic acid hydrochloride and 5.00 ml of thionyl chloride is allowed to stand at ambient temperature for 20 hours and then is concentrated in vacuo to yield 4-(n-hexadecylamino)benzoyl chloride hydrochloride as an orange solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04146546 |
| Source dataset | uspto-grants-1979_03 |
| ORD ID | ord-14331f94204e4190a4b3c5f5f11a0a63 |
| Source note | uspto-grants-1979_03 |