HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Ethyl Ketone → HCID 13454041, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Ethyl Ketone | HCID 6569 | — |
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Reactant | 2-Aminobenzimidazole | HCID 13624 | — |
| Product | HCID 13454041 | HCID 13454041 | — |
Reaction Steps
The title compound was prepared from 2-aminobenzimidazole, methyl ethyl ketone and methyl isocyanate employing the procedure of the first paragraph of Example 1. The product was purified by column chromatography, developing with chloroform/methanol (97%/2.4% by volume), giving a tan solid, mp 113°-119° C. (dec.). The confirmatory elemental analysis is shown in Table III.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04497650 |
| Source dataset | uspto-grants-1985_02 |
| ORD ID | ord-ab65fba3580e47ec9ef556652734171c |
| Source note | uspto-grants-1985_02 |