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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 615086Generated: October 31, 2026

Isopropyl isocyanate → 1,3,5-Triazino(1,2-a)benzimidazole-10(2H)-carboxamide,3,4-dihydro-2,2,3-trimethyl-N-(1-methylethyl)-4-oxo-

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Reaction equation

Participants

RoleNameHCIDCharge
ReactantIsopropyl isocyanateHCID 61277—
Reactant1,2-dihydro-2,2,3-trimethyl-1,3,5-triazino[1,2-a]benzimidazol-4(3H)-oneHCID 159120—
Product1,3,5-Triazino(1,2-a)benzimidazole-10(2H)-carboxamide,3,4-dihydro-2,2,3-trimethyl-N-(1-methylethyl)-4-oxo-HCID 159109—

Reaction Steps

The procedure of Example 10 was used to prepare the title compound from 1,2-dihydro-2,2,3-trimethyl-1,3,5-triazino[1,2-a]benzimidazol-4(3H)-one and isopropyl isocyanate. The product crystallized as a white solid, mp 93°-96° C. The confirmatory elemental analysis is shown in Table III.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04497650
Source datasetuspto-grants-1985_02
ORD IDord-eacc520e0be746da8ab0f35aff7af610
Source noteuspto-grants-1985_02