HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropyl isocyanate → 1,3,5-Triazino(1,2-a)benzimidazole-10(2H)-carboxamide,3,4-dihydro-2,2,3-trimethyl-N-(1-methylethyl)-4-oxo-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropyl isocyanate | HCID 61277 | — |
| Reactant | 1,2-dihydro-2,2,3-trimethyl-1,3,5-triazino[1,2-a]benzimidazol-4(3H)-one | HCID 159120 | — |
| Product | 1,3,5-Triazino(1,2-a)benzimidazole-10(2H)-carboxamide,3,4-dihydro-2,2,3-trimethyl-N-(1-methylethyl)-4-oxo- | HCID 159109 | — |
Reaction Steps
The procedure of Example 10 was used to prepare the title compound from 1,2-dihydro-2,2,3-trimethyl-1,3,5-triazino[1,2-a]benzimidazol-4(3H)-one and isopropyl isocyanate. The product crystallized as a white solid, mp 93°-96° C. The confirmatory elemental analysis is shown in Table III.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04497650 |
| Source dataset | uspto-grants-1985_02 |
| ORD ID | ord-eacc520e0be746da8ab0f35aff7af610 |
| Source note | uspto-grants-1985_02 |