Benzo(d)thiazol-2-amine → HCID 12926125, compound

Participants

Reaction Steps

To 70 ml of methyl ethyl ketone were added 7 g of 2-aminobenzothiazole and 10 g of o-methoxyphenacyl bromide and the mixture was refluxed for 10 hours. The reaction mixture was filtered while it was hot to recover crystals precipitated. The crystals were washed with methyl ethyl ketone, and dried to provide 3.0 g of 2-(o-methoxyphenyl)imidazo[2,1-b]-benzothiazole hydrobromide having a melting point of 263°-265° C.

Provenance & Evidence