HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bis(2-ethylhexyl)amine → 2-chloro-N,N-bis(2-ethylhexyl)-2-phenyl-acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bis(2-ethylhexyl)amine | HCID 7791 | — |
| Reactant | Chloro(phenyl)acetyl chloride | HCID 102902 | — |
| Product | 2-chloro-N,N-bis(2-ethylhexyl)-2-phenyl-acetamide | HCID 118059549 | 96% |
Reaction Steps
Step A is conducted starting from 2,2′-diethylhexylamine and α-chlorophenylacetyl chloride and leads to 2-chloro-N,N-bis(2-ethylhexyl)-2-phenyl-acetamide (Yield: 96%) for which the characterisations by 1H and 13C NMR are given below:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09441285B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-0e9e4199149b43188a2b7b866cc8e30c |
| Source note | uspto-grants-2016_09 |