2-Chlorobenzoyl isocyanate → HCID 13229716, compound

Participants

Reaction Conditions

Reaction Steps

A solution of 3.6 g of 2-chlorobenzoyl isocyanate in 20 ml of dry toluene was added to a stirred solution of 3.75 g of N-[4-(trifluoromethoxy)phenyl]-2,4-dinitrobenzenesulphenamide in 30 ml of the same solvent at room temperature. After 6 days, the reaction mixture was cooled to -5° C. and filtered, washed with cold toluene and with cold light petroleum (b.p. 40°-60° C.) to give 2, as pale yellow crystals, m.p.: 184°-186° C. (with decomposition).

Provenance & Evidence