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HRID61525

反应详情

EQUATION

反应方程式

HRID 61525 的结构方程式

REACTANTS

反应物

3
结构：COc1ccc([C@@H]2CC(=O)c3c(O)cc(O[C@@H]4O[C@H](CO[C@@H]5O[C@@H](C)[C@H](O)[C@@H](O)[C@H]5O)[C@@H](O)[C@H](O)[C@H]4O)cc3O2)cc1O
HCID10621

Hesperidin

C28H34O15

3 次

结构：[Na+].[OH-]
HCID14798

Sodium Hydroxide

HNaO

结构：[Ag]
HCID23954

Silver

Ag

PRODUCTS

生成物

1
结构：COc1ccc([C@@H]2CC(=O)c3c(O)cc(O[C@@H]4O[C@H](CO[C@@H]5O[C@@H](C)[C@H](O)[C@@H](O)[C@H]5O)[C@@H](O)[C@H](O)[C@H]4O)cc3O2)cc1O.[Ag]
HCID131737181

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：O
溶剂HCID962

Water

H2O

2 次

结构：Cc1ccc(S(=O)(=O)[O-])cc1.[Ag+]
溶剂HCID85606

Silver p-toluenesulphonate

C7H7AgO3S

PROCEDURE

实验过程

Hesperidin/silver colloidal nanoparticle catalyst is prepared by dissolving 1.65 g hesperidin in a beaker containing 800 ml DI water at room temperature. 1 N NaOH solution with stirring is added to adjust the solution pH to 11. In a separate beaker, 2.2 g silver p-toluenesulfonate is dissolved in 60 ml DI water. The silver ion solution is added to the hesperidin solution with strong stirring. The molar ratio of silver to hesperidin is 1:0.34. The beaker containing the aqueous catalyst solution is placed in a 50° C. water bath for 12 hours to test its stability. After 12 hours the solution is observed and no precipitate is expected indicating that the catalyst is still stable.

WORKUP

后处理

  1. additionis added
  2. additionThe beaker containing the aqueous catalyst solution
  3. customis placed in a 50° C.
  4. customfor 12 hours