HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorophenyl Isocyanate → N-(4-Chlorophenyl)-4-oxo-2,3,4,10-tetrahydro-2,2,3-trimethyl-1,3,5-triazino[1,2-a]benzimidazole-10-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorophenyl Isocyanate | HCID 7693 | — |
| Reactant | 1,2-dihydro-2,2,3-trimethyl-1,3,5-triazino[1,2-a]benzimidazol-4(3H)-one | HCID 159120 | — |
| Product | N-(4-Chlorophenyl)-4-oxo-2,3,4,10-tetrahydro-2,2,3-trimethyl-1,3,5-triazino[1,2-a]benzimidazole-10-carboxamide | HCID 13454044 | — |
Reaction Steps
The procedure of Example 10 was used to prepare the title compound from 1,2-dihydro-2,2,3-trimethyl-1,3,5-triazino[1,2-a]benzimidazol-4(3H)-one and 4-chlorophenyl isocyanate. The confirmatory elemental analysis for the product, mp 206°-211° C., is shown in Table III.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04498920 |
| Source dataset | uspto-grants-1985_02 |
| ORD ID | ord-aeb3968c2a5a426c953f25bac6eda0db |
| Source note | uspto-grants-1985_02 |