huagongshe.com
HRID615303

反应详情

EQUATION

反应方程式

HRID 615303 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OOC(=O)c1ccc(C(=O)c2ccccc2)cc1
HCID13494638

tert-Butyl 4-benzoylbenzene-1-carboperoxoate

C18H18O4

结构：CCCC(=O)c1ccc(C(=O)O)cc1
HCID18983564

未命名化合物

PRODUCTS

生成物

1
结构：CCCC(=O)c1ccc(C(=O)OOC(C)(C)C)cc1
HCID85977582

未命名化合物

PROCEDURE

实验过程

Tert-butyl-ρ-butyrylperbenzoate is prepared by the above-discussed procedure for the preparation of t-butyl-4-benzoylperbenzoate, except that the acid employed is ρ-butyryl benzoic acid and is purified by chromatography over neutral aluminum oxide with dichloromethane-ether (5:1) as eluent. The perester obtained is a yellow oil which solidifies after several months in the refrigerator.

WORKUP

后处理

  1. customis purified by chromatography over neutral aluminum oxide with dichloromethane-ether (5:1) as eluent
  2. customThe perester obtained
  3. waitsolidifies after several months in the refrigerator