Ethylene Glycol → HCID 20427335, compound

HRID 615305Notes

Reaction equation

[CH:1]1([CH:7]2[CH2:12][CH2:11][CH2:10][CH2:9][C:8]2=[O:13])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.COC(OC)OC.[CH2:21](O)[CH2:22][OH:23]>>[CH:1]1([CH:7]2[CH2:12][CH2:11][CH2:10][CH2:9][C:8]32[O:23][CH2:22][CH2:21][O:13]3)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6]1

Participants

Reactant 3

HCID 174Ethylene Glycol

HCID 70161,1'-Bi(cyclohexyl)-2-one

HCID 9005Trimethyl orthoformate

Product 1

HCID 20427335HCID 20427335, compound

Procedure

1,260 g (7 mols) of 2-cyclohexyl-cyclohexanone are reacted with 816.2 g (7.7 mols) of trimethylorthoformate and 477.4 g (7.7 mols) of anhydrous 1,2-ethanediol in a manner analogous to that in Example 1.

Sources & evidence

ORD record: ord-96d0c3d5ef584597aecd70c9db2f2e9d
Source dataset: uspto-grants-1985_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04499000

Reaction notes

Loading…