1,1'-Bi(cyclohexyl)-2-one → HCID 15607005, compound

HRID 615306Notes

Reaction equation

[CH:1]1([CH:7]2[CH2:12][CH2:11][CH2:10][CH2:9][C:8]2=[O:13])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.C(OC)(OC)OC.[CH3:21][C:22]([CH3:27])([CH2:25]O)[CH2:23][OH:24]>>[CH:1]1([CH:7]2[CH2:12][CH2:11][CH2:10][CH2:9][C:8]32[O:24][CH2:23][C:22]([CH3:27])([CH3:25])[CH2:21][O:13]3)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6]1

Participants

Reactant 3

HCID 70161,1'-Bi(cyclohexyl)-2-one

HCID 9005Trimethyl orthoformate

HCID 31344Neopentyl glycol

Product 1

HCID 15607005HCID 15607005, compound

Procedure

1.170 g (6.5 mols) of 2-cyclohexyl-cyclohexanone are reacted with 757.9 g (7.15 mols) of trimethyl orthoformate and 743.6 g (7.15 mols) of anhydrous 2,2-dimethyl-1,3-propanediol in a manner analogous to that in Example 1:

Sources & evidence

ORD record: ord-a3dc9908ac2d4dfcb9dd8562a7113be6
Source dataset: uspto-grants-1985_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04499000

Reaction notes

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