HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 13365266, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 3-(Dimethylamino)propyl chloride hydrochloride | HCID 94308 | — |
| Reactant | HCID 13236221 | HCID 13236221 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 13365266 | HCID 13365266 | — |
Reaction Steps
A suspension of 10.0 g 2-isopropylthio-5-oxo-4,4-diphenyl-2-pyrroline-3-carbonitrile and 0.9 g sodium hydride (80%) in 150 ml dioxan is boiled for one hour, with stirring. Thereafter, one mixes with a further 0.9 g sodium hydride and 5.2 g dimethylaminopropyl chloride hydrochloride and boils further for 30 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04499089 |
| Source dataset | uspto-grants-1985_02 |
| ORD ID | ord-383d41f036cc4c75951a22dafbb0137d |
| Source note | uspto-grants-1985_02 |