HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-{[(3-Bromopyridin-2-yl)methyl]sulfanyl}ethan-1-amine → HCID 178512223, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-{[(3-Bromopyridin-2-yl)methyl]sulfanyl}ethan-1-amine | HCID 12951527 | — |
| Reactant | N-benzoyl-N',N"-bis-[2-((3-bromo-2-pyridyl)methylthio)ethyl]guanidine | HCID 54262795 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 178512223 | HCID 178512223 | — |
Reaction Steps
The reaction of 3-bromo-2-[(2-aminoethyl)thiomethyl]pyridine with N-benzoyl-bis-dimethylthioimidocarbonate in pyridine by the method described in Example 12 yielded N-benzoyl-N',N"-bis-[2-((3-bromo-2-pyridyl)methylthio)ethyl]guanidine which, on acid hydrolysis, yielded the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04499101 |
| Source dataset | uspto-grants-1985_02 |
| ORD ID | ord-fc5b10c86a4e482cad9f8469fa305b39 |
| Source note | uspto-grants-1985_02 |