HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → N-(Butan-2-yl)-N-methyl-4-phenylnaphthalene-2-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | N-Methyl-2-butanamine | HCID 111026 | — |
| Reactant | 4-Phenylnaphthalene-2-carboxylic acid | HCID 13272348 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | N-(Butan-2-yl)-N-methyl-4-phenylnaphthalene-2-carboxamide | HCID 13272352 | 54.9% |
Reaction Steps
Operations are carried out as for Example 1, starting from 4.3 g of 4-phenyl naphthalene 2-carboxylic acid, 20 ml of thionyl chloride and then 1.5 g of N-methyl 2-butanamine in 20 ml of pyridine. 3 g of N-methyl N(1-methyl propyl) 4-phenyl naphthalene 2-carboxamide, melting at 108° C., are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04499094 |
| Source dataset | uspto-grants-1985_02 |
| ORD ID | ord-489f312cf48c49a8af7936658bcd88e4 |
| Source note | uspto-grants-1985_02 |