HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → N,N-Diethyl-4-phenylquinazoline-2-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-Phenylquinazoline-2-carboxylic acid | HCID 3738719 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | N,N-Diethyl-4-phenylquinazoline-2-carboxamide | HCID 13272356 | — |
Reaction Steps
Operations are carried out as for Example 19, starting from 2.5 g of 4-phenyl quinazoline 2-carboxylic acid, 10 ml of thionyl chloride 25 ml of toluene and 25 ml of diethylamine. 1.27 g of N,N-diethyl 4-phenyl quinazoline 2-carboxamide, melting at 101° C., is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04499094 |
| Source dataset | uspto-grants-1985_02 |
| ORD ID | ord-3d8dc96cd02c4866829b0a57e04aca70 |
| Source note | uspto-grants-1985_02 |