HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 24845779, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 53821249 | HCID 53821249 | — |
| Product | HCID 24845779 | HCID 24845779 | — |
Reaction Steps
Operations are carried out as for Example 1, starting from 21 g of 4-(4-methoxy phenyl) quinoline 2-carboxylic acid, 64 ml of thionyl chloride and 39 ml of diethylamine. 2.2 g of N,N-diethyl 4-(4-methoxy phenyl) quinoline 2-carboxamide are obtained. After recrystallization in isopropyl ether the product melts at 91° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04499094 |
| Source dataset | uspto-grants-1985_02 |
| ORD ID | ord-aad68ab85414409da616e4fd1f8e3910 |
| Source note | uspto-grants-1985_02 |