Nitric Acid → HCID 53948822, compound

HRID 615406Notes

Reaction equation

HRID 615406 reaction equation
[CH3:1][C:2]1[CH:11]=[C:10]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[N:3]=1.[N+:18]([O-])([OH:20])=[O:19]>S(=O)(=O)(O)O>[CH3:1][C:2]1[CH:11]=[C:10]([C:12]2[CH:17]=[CH:16][CH:15]=[C:14]([N+:18]([O-:20])=[O:19])[CH:13]=2)[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[N:3]=1

Participants

4

Reactant 2

HCID 944Nitric AcidHCID 6130202-Methyl-4-phenylquinoline

Product 1

HCID 53948822HCID 53948822, compound

Reagents, catalysts & solvents 1

HCID 1118Sulfuric AcidSolvent

Procedure

2-methyl 4-(3-nitro phenyl) quinoline is prepared by nitration at 0° C. of 2-methyl 4-phenyl quinoline (1.36 10-1 mole) with sulfonitric mixture (90 ml nitric acid 60% and 90 ml concentrated sulfuric acid) and separation of isomers. It has a melting point of 157° C.

Sources & evidence

ORD record
ord-e827bcdf51164c10b0d9a84f66a1f53a
Source dataset
uspto-grants-1985_02
Patent number
US04499094

Reaction notes

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