HRID615501

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6367

Acetyl chloride

C2H3ClO

HCID15835

4-Methylcinnamic acid

C10H10O2

PRODUCTS

生成物

HCID589472

Methyl 3-(4-methylphenyl)-2-propenoate

C11H12O2

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

A solution of 6.0 g (37.0 mmol) of 4-methylcinnamic acid in 120 ml of anhydrous MeOH was treated with 6 ml of acetyl chloride and stirred at reflux for 18 hours. Evaporation of the MeOH gave the title ester as a white solid, mp 53.5°-57.5° C.

WORKUP

后处理

temperatureat reflux for 18 hours
customEvaporation of the MeOH