HCID 53812018, compound → HCID 54236840, compound

HRID 615509Notes

Reaction equation

HRID 615509 reaction equation
CC1C=C(C=CC=1OC)C=CC(OC)=O.[CH3:16][O:17][C:18]1[CH:29]=[CH:28][C:21]([CH:22]=[CH:23][C:24]([O:26]C)=[O:25])=[CH:20][C:19]=1[CH2:30][O:31][C:32]1[CH:37]=[CH:36][C:35]([C:38](=[O:40])[CH3:39])=[C:34]([OH:41])[C:33]=1[CH2:42][CH2:43][CH3:44]>>[CH3:16][O:17][C:18]1[CH:29]=[CH:28][C:21]([CH:22]=[CH:23][C:24]([OH:26])=[O:25])=[CH:20][C:19]=1[CH2:30][O:31][C:32]1[CH:37]=[CH:36][C:35]([C:38](=[O:40])[CH3:39])=[C:34]([OH:41])[C:33]=1[CH2:42][CH2:43][CH3:44]

Participants

3

Reactant 2

HCID 53812018HCID 53812018, compoundHCID 54403318HCID 54403318, compound

Product 1

HCID 54236840HCID 54236840, compound

Procedure

Methyl 3-methyl-4-methoxycinnamate was carried through steps analogous to those described in Example 16, steps b., c. and d. Methyl 4-methoxy-3-(4-acetyl-3-hydroxy-2-propylphenoxy)methylcinnamate melted at 141°-143° C. The title compound was recrystallized from ethanol to give flocculent needles, mp 245°-246° C.

Workup

  1. customThe title compound was recrystallized from ethanol
  2. customto give flocculent needles, mp 245°-246° C.

Sources & evidence

ORD record
ord-af6dca2e67c94c7b8383abb02df2eeb9
Source dataset
uspto-grants-1985_02
Patent number
US04499299

Reaction notes

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