HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Methylhydroxylamine → N-(5-tert-Butyl-1,2-oxazol-3-yl)-N'-methoxyurea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Methylhydroxylamine | HCID 4113 | — |
| Reactant | 5-Tert-butyl-3-isocyanato-1,2-oxazole | HCID 12918838 | — |
| Product | N-(5-tert-Butyl-1,2-oxazol-3-yl)-N'-methoxyurea | HCID 13370466 | — |
Reaction Steps
8.5 g of methoxyamine was added slowly to a stirred solution of 15 g of 3A in 600 ml of tetrahydrfuran. The resulting mixture was filtered and the solid was triturated with ether to give 1-methoxy-3-(5-(1,1-dimethylethyl)-isoxazol-3-yl)urea (3B), m.p.: 145°-148° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04500345 |
| Source dataset | uspto-grants-1985_02 |
| ORD ID | ord-5485056bf3234899a13d46d5ae47cd16 |
| Source note | uspto-grants-1985_02 |