HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroform → HCID 47000767, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | Isopropylamine | HCID 6363 | — |
| Reactant | Benzene, (2-bromoethoxy)- | HCID 68526 | — |
| Product | HCID 47000767 | HCID 47000767 | — |
Reaction Steps
Following the procedure of Preparation 1, 2-bromoethyl phenyl ether and isopropyl amine were reacted (in refluxing chloroform) overnight and the reaction mixture processed to yield an oil, the free base of the title compound. A portion of the oil was reacted with ethereal hydrogen chloride to form the hydrochloride salt in 68.3% yield, m.p. 152°-154.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04500529 |
| Source dataset | uspto-grants-1985_02 |
| ORD ID | ord-bf5ba87cec534b8f89ad9e3e9699b6bd |
| Source note | uspto-grants-1985_02 |