HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 615653Generated: October 30, 2026
1-Bromohexadecane → HCID 12886752, compound
https://huagongshe.com/reaction/615653
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1-Bromohexadecane | HCID 8213 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Methyl-1,3-benzoxazol-6-ol | HCID 676504 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 12886752 | HCID 12886752 | 100.5% |
Reaction Steps
A mixture of 18.0 g of 6-hydroxy-2-methylbenzoxazole, 36.6 g of 1-bromohexadecane, 24.0 g of potassium carbonate and 120 ml of N,N-dimethylformamide was stirred at 90° C. for 4.5 hours. The reaction solution was filtered to remove solids and the filtrate was poured into 500 ml of methanol to precipitate crystals. These crystals were collected by filtration. 45.0 g of 6-hexadecyloxy-2-methylbenzoxazole was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04500626 |
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| Source dataset | uspto-grants-1985_02 |
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| ORD ID | ord-71cf8c853b3444c9a27075aae9944732 |
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| Source note | uspto-grants-1985_02 |
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