HCID 53969683, compound → HCID 54165185, compound

HRID 615685Notes

Reaction equation

HRID 615685 reaction equation
[C:1]([S:9][C@@H:10]([CH2:35][S:36][C:37](=[O:44])[C:38]1[CH:43]=[CH:42][CH:41]=[CH:40][CH:39]=1)[C:11]([NH:13][C@H:14]([C:18]([NH:20][C@H:21]([C:32]([OH:34])=[O:33])[CH2:22][C:23]1C2C(=CC=CC=2)N[CH:24]=1)=[O:19])[CH:15]([CH3:17])[CH3:16])=[O:12])(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1>C1(C)C=CC=CC=1>[C:1]([S:9][C@H:10]([CH2:35][S:36][C:37](=[O:44])[C:38]1[CH:39]=[CH:40][CH:41]=[CH:42][CH:43]=1)[C:11]([NH:13][C@H:14]([C:18]([N:20]1[CH2:24][CH2:23][CH2:22][C@H:21]1[C:32]([OH:34])=[O:33])=[O:19])[CH:15]([CH3:16])[CH3:17])=[O:12])(=[O:8])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 1

HCID 53969683HCID 53969683, compound

Product 1

HCID 54165185HCID 54165185, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

N-[(R)-2,3-Bis-(benzoylthio)-propionyl]-valyltryptophan, melting point 205°-208° C. (toluene), Rf=0.60 in system I.

Sources & evidence

ORD record
ord-900811d4e55847b8a8a13aaddad77e44
Source dataset
uspto-grants-1985_02
Patent number
US04500467

Reaction notes

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