Sodium Hydroxide → HCID 178461623, compound
Reaction equation
Cl[Ge:2]([CH3:17])([Ge:10]([CH2:15][CH3:16])([CH2:13][CH3:14])[CH2:11][CH3:12])[Ge:3]([CH2:8][CH3:9])([CH2:6][CH3:7])[CH2:4][CH3:5].[OH-:18].[Na+]>O>[O:18]([Ge:2]([CH3:17])([Ge:10]([CH2:13][CH3:14])([CH2:15][CH3:16])[CH2:11][CH3:12])[Ge:3]([CH2:6][CH3:7])([CH2:4][CH3:5])[CH2:8][CH3:9])[Ge:2]([CH3:17])([Ge:10]([CH2:15][CH3:16])([CH2:13][CH3:14])[CH2:11][CH3:12])[Ge:3]([CH2:8][CH3:9])([CH2:6][CH3:7])[CH2:4][CH3:5]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
This compound was prepared according to the process described in Example I, starting from 3.0 g of 2-chloro-2-methylhexaethyltrigermane, 0.6 g of sodium hydroxide and 3 ml of water. 3.1 g (55%) of colorless, liquid oxybis(1,1,1,3,3,3-hexaethylmethyltrigermane) were obtained; nD20 =1.5410.
Workup
- customThis compound was prepared
Sources & evidence
- ORD record
- ord-a4ee6f2c30ac4704956e018ad906151b
- Source dataset
- uspto-grants-1985_02
- Patent number
- US04501702
Reaction notes
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