Propanamide, 2-chloro-N,N-dimethyl- → HCID 20370343, compound

HRID 615960Notes

Reaction equation

HRID 615960 reaction equation
C[C:2]1[C:3]([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=2)=[N:4][NH:5][CH:6]=1.Br[CH:14]([CH2:20][CH3:21])[C:15]([N:17]([CH3:19])[CH3:18])=[O:16].[Cl:22]C(C)C(N(C)C)=O>>[Cl:22][C:12]1[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=1[C:3]1[CH:2]=[CH:6][N:5]([CH:14]([CH2:20][CH3:21])[C:15]([N:17]([CH3:19])[CH3:18])=[O:16])[N:4]=1

Participants

4

Reactant 3

HCID 112034Propanamide, 2-chloro-N,N-dimethyl-HCID 30160612-Bromo-N,N-dimethylbutanamideHCID 178430907HCID 178430907, compound

Product 1

HCID 20370343HCID 20370343, compound

Procedure

Following the procedure of Example 1, but substituting 3-(o-chlorophenyl)pyrazole for 4-methyl-3-phenylpyrazole and 2-bromo-N,N-dimethylbutyramide for 2-chloro-N,N-dimethylpropionamide there was obtained 3-(o-chlorophenyl)-α-ethyl-N,N-dimethylpyrazole-1-acetamide having a melting point of 38.5°-40° C.

Sources & evidence

ORD record
ord-af9d3f8589694bcda8b485beaa899859
Source dataset
uspto-grants-1978_02
Patent number
US04072498

Reaction notes

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