Propanamide, 2-chloro-N,N-dimethyl- → alpha-cyclohexyl-N,N-dimethyl-3-phenylpyrazole-1-acetamide

HRID 615964Notes

Reaction equation

HRID 615964 reaction equation
Cl[CH:2]([CH3:8])[C:3]([N:5]([CH3:7])[CH3:6])=[O:4].[C:9]1([C:15]2[CH:19]=[CH:18][NH:17][N:16]=2)[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1.[CH3:20][C:21]1[C:22]([C:26]2C=CC=C[CH:27]=2)=NNC=1>>[CH:8]1([CH:2]([N:17]2[CH:18]=[CH:19][C:15]([C:9]3[CH:10]=[CH:11][CH:12]=[CH:13][CH:14]=3)=[N:16]2)[C:3]([N:5]([CH3:7])[CH3:6])=[O:4])[CH2:27][CH2:26][CH2:22][CH2:21][CH2:20]1

Participants

4

Reactant 3

HCID 112034Propanamide, 2-chloro-N,N-dimethyl-HCID 178420101HCID 178420101, compoundHCID 178430907HCID 178430907, compound

Product 1

HCID 20370491alpha-cyclohexyl-N,N-dimethyl-3-phenylpyrazole-1-acetamide

Procedure

Following the procedure of Example 1, but substituting α-bromo-N,N-dimethyl-1-cyclohexaneacetamide for 2-chloro N,N-dimethylpropionamide and 3-phenylpyrazole for 4-methyl-3-phenylpyrazole there was obtained α-cyclohexyl-N,N-dimethyl-3-phenylpyrazole-1-acetamide having a melting point of 87.5°-90° C.

Sources & evidence

ORD record
ord-f66e288e751740f291912d5746a3085b
Source dataset
uspto-grants-1978_02
Patent number
US04072498

Reaction notes

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