Ammonia → HCID 20370577, compound

HRID 615968Notes

Reaction equation

HRID 615968 reaction equation
N.[CH3:2][C:3]1[C:4]([C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)=[N:5][N:6]([CH:8]([CH2:12][CH2:13][CH3:14])[C:9]([OH:11])=O)[CH:7]=1.[CH3:21][CH:22]([N:26]1[CH:30]=[C:29](C)C(C2C=CC=CC=2)=N1)C(O)=O>>[CH2:22]([N:26]([CH2:30][CH3:29])[C:9](=[O:11])[CH:8]([CH2:12][CH2:13][CH3:14])[N:6]1[CH:7]=[C:3]([CH3:2])[C:4]([C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)=[N:5]1)[CH3:21]

Participants

4

Reactant 3

HCID 222AmmoniaHCID 20370468alpha,4-Dimethyl-3-phenyl-1H-pyrazole-1-acetic acidHCID 53897824HCID 53897824, compound

Product 1

HCID 20370577HCID 20370577, compound

Procedure

Following the procedure of Example 68, but substituting diethylamine for aqueous ammonia and 4-methyl-3-phenyl-α-propylpyrazole-1-acetic acid for α,4-dimethyl-3-phenylpyrazole-1-acetic acid, there was obtained N,N-diethyl-4-methyl-3-phenyl-α-propylpyrazole-1acetamide having a melting point of 65°-67° C.

Sources & evidence

ORD record
ord-2a16a8a494414b258f742427a92eedee
Source dataset
uspto-grants-1978_02
Patent number
US04072498

Reaction notes

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