HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Tetrachloride → 2-(4-Chloro-3-phenyl-1H-pyrazol-1-yl)-N,N,2-trimethylpropanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Tetrachloride | HCID 5943 | — |
| Reactant | Bromine | HCID 24408 | — |
| Reactant | Tert-Butyl hypochlorite | HCID 521297 | — |
| Reactant | N,N-Dimethyl-2-(5-methyl-3-phenyl-1H-pyrazol-1-yl)propanamide | HCID 20370380 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 2-(4-Chloro-3-phenyl-1H-pyrazol-1-yl)-N,N,2-trimethylpropanamide | HCID 20370505 | — |
Reaction Steps
Following the procedure of Example 108, but substituting N,N,α,α-tetramethyl-3-phenylpyrazole-1-acetamide for N,N,α,5-tetramethyl-3-phenylpyrazole-1-acetamide, tert-butyl hypochlorite for bromine, and carbon tetrachloride for acetic acid as the reaction solvent, there was obtained 4-chloro-N,N,α,α-tetramethyl-3-phenylpyrazole-1-acetamide having a melting point of 117°-119° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04072498 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-4c14f1aadbf34c71ae0d8d69bba1f7a0 |
| Source note | uspto-grants-1978_02 |