Propanamide, 2-chloro-N,N-dimethyl- → HCID 20370457, compound

HRID 615985Notes

Reaction equation

Cl[CH:2]([CH3:8])[C:3]([N:5]([CH3:7])[CH3:6])=[O:4].[CH3:9][C:10]1[C:11]([C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)=[N:12][NH:13][C:14]=1[CH3:15].[CH3:22]C1C(C2C=CC=CC=2)=NNC=1>>[CH2:8]([CH:2]([N:13]1[C:14]([CH3:15])=[C:10]([CH3:9])[C:11]([C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)=[N:12]1)[C:3]([N:5]([CH3:7])[CH3:6])=[O:4])[CH3:22]

Participants

Reactant 3

HCID 112034Propanamide, 2-chloro-N,N-dimethyl-

HCID 2753112ZINC03848355

HCID 178430907HCID 178430907, compound

Product 1

HCID 20370457HCID 20370457, compound

Procedure

Using the procedure of Example 1, but substituting 2-bromo-N,N-dimethylbutyramide for 2-chloro-N,N-dimethylpropionamide and 4,5-dimethyl-3-phenylpyrazole for 4-methyl-3-phenylpyrazole there was obtained α-ethyl-N,N,4,5-tetramethyl-3-phenylpyrazole-1-acetamide, m.p. 119°-121° C.

Sources & evidence

ORD record: ord-8b7eedf1b4e7413398c2f348d3e9382d
Source dataset: uspto-grants-1978_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04072498

Reaction notes

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