Propanamide, 2-chloro-N,N-dimethyl- → HCID 20370441, compound

HRID 615986Notes

Reaction equation

HRID 615986 reaction equation
Cl[CH:2]([CH3:8])[C:3]([N:5]([CH3:7])[CH3:6])=[O:4].[CH2:9]([C:11]1[C:12]([C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)=[N:13][NH:14][CH:15]=1)[CH3:10].[CH3:22]C1C(C2C=CC=CC=2)=NNC=1>>[CH2:8]([CH:2]([N:14]1[CH:15]=[C:11]([CH2:9][CH3:10])[C:12]([C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)=[N:13]1)[C:3]([N:5]([CH3:7])[CH3:6])=[O:4])[CH3:22]

Participants

4

Reactant 3

HCID 112034Propanamide, 2-chloro-N,N-dimethyl-HCID 178430907HCID 178430907, compoundHCID 178437209HCID 178437209, compound

Product 1

HCID 20370441HCID 20370441, compound

Procedure

Using the procedure of Example 1, but substituting 2-bromo-N,N-dimethylbutyramide for 2-chloro-N,N-dimethylpropionamide and 4-ethyl-3-phenylpyrazole for 4-methyl-3-phenylpyrazole, there was obtained α,4-diethyl-N,N-dimethyl-3-phenylpyrazole-1-acetamide, m.p. 77.5°-79° C.

Sources & evidence

ORD record
ord-5fdeeb4c82bb43988fd99ca2f8efd91c
Source dataset
uspto-grants-1978_02
Patent number
US04072498

Reaction notes

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