Propanamide, 2-chloro-N,N-dimethyl- → HCID 20370433, compound

HRID 615987Notes

Reaction equation

HRID 615987 reaction equation
Cl[CH:2]([CH3:8])[C:3]([N:5]([CH3:7])[CH3:6])=[O:4].[Cl:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[C:16]1[C:20]([CH2:21][CH3:22])=[CH:19][NH:18][N:17]=1.[CH3:23]C1C(C2C=CC=CC=2)=NNC=1>>[Cl:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[C:16]1[C:20]([CH2:21][CH3:22])=[CH:19][N:18]([CH:2]([CH2:8][CH3:23])[C:3]([N:5]([CH3:7])[CH3:6])=[O:4])[N:17]=1

Participants

4

Reactant 3

HCID 112034Propanamide, 2-chloro-N,N-dimethyl-HCID 178430907HCID 178430907, compoundHCID 178437210HCID 178437210, compound

Product 1

HCID 20370433HCID 20370433, compound

Procedure

Using the procedure for Example 1, but substituting 2-bromo-N,N-dimethylbutyramide for 2-chloro-N,N-dimethylpropionamide and 3-(o-chlorophenyl)-4-ethylpyrazole for 4-methyl-3-phenylpyrazole, there was obtained 3-(o-chlorophenyl)-α,4-diethyl-N,N-dimethylpyrazole-1-acetamide, m.p. 60°-63° C.

Sources & evidence

ORD record
ord-adc01a4df6ce4ecf9c3991ec430bd5fd
Source dataset
uspto-grants-1978_02
Patent number
US04072498

Reaction notes

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