Propanamide, 2-chloro-N,N-dimethyl- → HCID 20370417, compound

HRID 615994Notes

Reaction equation

HRID 615994 reaction equation
Cl[CH:2]([CH3:8])[C:3]([N:5]([CH3:7])[CH3:6])=[O:4].[CH3:9][C:10]1[C:11]([C:15]2[CH:20]=[CH:19][C:18]([CH3:21])=[CH:17][C:16]=2[CH3:22])=[N:12][NH:13][CH:14]=1.[CH3:23]C1C(C2C=CC=CC=2)=NNC=1>>[CH2:8]([CH:2]([N:13]1[CH:14]=[C:10]([CH3:9])[C:11]([C:15]2[CH:20]=[CH:19][C:18]([CH3:21])=[CH:17][C:16]=2[CH3:22])=[N:12]1)[C:3]([N:5]([CH3:7])[CH3:6])=[O:4])[CH3:23]

Participants

4

Reactant 3

HCID 112034Propanamide, 2-chloro-N,N-dimethyl-HCID 178424077HCID 178424077, compoundHCID 178430907HCID 178430907, compound

Product 1

HCID 20370417HCID 20370417, compound

Procedure

Using the procedure of Example 1, but substituting 2-bromo-N,N-dimethylbutyramide for 2-chloro-N,N-dimethylpropionamide and 4-methyl-3-(2,4-dimethylphenyl)pyrazole for 4-methyl-3-phenylpyrazole there is obtained α-ethyl-N,N,4-trimethyl-3-(2,4-dimethylphenyl)pyrazole-1-acetamide isolated as an oil.

Sources & evidence

ORD record
ord-54411d7b99514281b75f3810574f3537
Source dataset
uspto-grants-1978_02
Patent number
US04072498

Reaction notes

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