Propanamide, 2-chloro-N,N-dimethyl- → HCID 20370569, compound

HRID 615995Notes

Reaction equation

HRID 615995 reaction equation
Cl[CH:2]([CH3:8])[C:3]([N:5]([CH3:7])[CH3:6])=[O:4].[CH3:9][O:10][C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][C:12]=1[C:17]1[C:21]([CH3:22])=[CH:20][NH:19][N:18]=1.[CH3:23]C1C(C2C=CC=CC=2)=NNC=1>>[CH2:8]([CH:2]([N:19]1[CH:20]=[C:21]([CH3:22])[C:17]([C:12]2[CH:13]=[CH:14][CH:15]=[CH:16][C:11]=2[O:10][CH3:9])=[N:18]1)[C:3]([N:5]([CH3:7])[CH3:6])=[O:4])[CH3:23]

Participants

4

Reactant 3

HCID 112034Propanamide, 2-chloro-N,N-dimethyl-HCID 178430907HCID 178430907, compoundHCID 178489419HCID 178489419, compound

Product 1

HCID 20370569HCID 20370569, compound

Procedure

Using the procedure of Example 1, but substituting 2-bromo-N,N-dimethylbutyramide for 2-chloro-N,N-dimethylpropionamide and 3-(o-methoxyphenyl)-4-methylpyrazole for 4-methyl-3-phenylpyrazole there is obtained α-ethyl-3-(o-methoxyphenyl)-N,N,4-trimethylpyrazole-1-acetamide, m.p. 79°-81° C.

Sources & evidence

ORD record
ord-934397995ae54d9aae3e6269be66b43a
Source dataset
uspto-grants-1978_02
Patent number
US04072498

Reaction notes

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