Propanamide, 2-chloro-N,N-dimethyl- → HCID 20370460, compound

HRID 615997Notes

Reaction equation

HRID 615997 reaction equation
Cl[CH:2]([CH3:8])[C:3]([N:5]([CH3:7])[CH3:6])=[O:4].[Cl:9][C:10]1[CH:15]=[CH:14][C:13]([C:16]2[C:20]([CH3:21])=[CH:19][NH:18][N:17]=2)=[C:12]([CH3:22])[CH:11]=1.[CH3:23]C1C(C2C=CC=CC=2)=NNC=1>>[Cl:9][C:10]1[CH:15]=[CH:14][C:13]([C:16]2[C:20]([CH3:21])=[CH:19][N:18]([CH:2]([CH2:8][CH3:23])[C:3]([N:5]([CH3:7])[CH3:6])=[O:4])[N:17]=2)=[C:12]([CH3:22])[CH:11]=1

Participants

4

Reactant 3

HCID 112034Propanamide, 2-chloro-N,N-dimethyl-HCID 178426100HCID 178426100, compoundHCID 178430907HCID 178430907, compound

Product 1

HCID 20370460HCID 20370460, compound

Procedure

Using the procedure of Example 1, but substituting 2-bromo-N,N-dimethylbutyramide for 2-chloro-N,N-dimethylpropionamide and 3-(4-chloro-2-methylphenyl)-4-methylpyrazole for 4-methyl-3-phenylpyrazole there is obtained 3-(4-chloro-2-methylphenyl)-α-ethyl-N,N,4-trimethylpyrazole-1-acetamide, m.p. 89°-92° C.

Sources & evidence

ORD record
ord-5e8f600dacdb443fb62d60dab21949cd
Source dataset
uspto-grants-1978_02
Patent number
US04072498

Reaction notes

Loading…