Propanamide, 2-chloro-N,N-dimethyl- → HCID 20370499, compound

HRID 615998Notes

Reaction equation

HRID 615998 reaction equation
Cl[CH:2]([CH3:8])[C:3]([N:5]([CH3:7])[CH3:6])=[O:4].[Cl:9][C:10]1[CH:15]=[C:14]([CH3:16])[CH:13]=[CH:12][C:11]=1[C:17]1[C:21]([CH3:22])=[CH:20][NH:19][N:18]=1.[CH3:23]C1C(C2C=CC=CC=2)=NNC=1>>[Cl:9][C:10]1[CH:15]=[C:14]([CH3:16])[CH:13]=[CH:12][C:11]=1[C:17]1[C:21]([CH3:22])=[CH:20][N:19]([CH:2]([CH2:8][CH3:23])[C:3]([N:5]([CH3:7])[CH3:6])=[O:4])[N:18]=1

Participants

4

Reactant 3

HCID 112034Propanamide, 2-chloro-N,N-dimethyl-HCID 178424078HCID 178424078, compoundHCID 178430907HCID 178430907, compound

Product 1

HCID 20370499HCID 20370499, compound

Procedure

Using the procedure of Example 1, but substituting 2-bromo-N,N-dimethylbutyramide for 2-chloro-N,N-dimethylpropionamide and 3-(2-chloro-4-methylphenyl)-4-methylpyrazole for 4-methyl-3-phenylpyrazole there is obtained 3-(2-chloro-4-methylphenyl)-α-ethyl-N,N,4-trimethylpyrazole-1-acetamide isolated as an oil.

Sources & evidence

ORD record
ord-a52812be48cf4e2699489f7624f87e9c
Source dataset
uspto-grants-1978_02
Patent number
US04072498

Reaction notes

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