HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 1-Acetamido-2-amino-4-benzylthiobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | N-[4-(Benzylsulfanyl)-2-nitrophenyl]acetamide | HCID 20362823 | — |
| Catalyst | Iron | HCID 23925 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 1-Acetamido-2-amino-4-benzylthiobenzene | HCID 20371189 | — |
Reaction Steps
2.4 G. of 1-acetamido-2-nitro-4-benzylthiobenzene is treated with 2.4 g. iron powder and 1.2 g. ferrous sulfate in a mixture of 60 ml. water and 240 ml. methanol, at reflux for 4 hours. The mixture is then filtered, the filtrate concentrated and the residue recrystallized from benzene. Pure 1-acetamido-2-amino-4-benzylthiobenzene is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04072696 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-1b56a93dea7345e5adf1da1fd8c48dbc |
| Source note | uspto-grants-1978_02 |