HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methoxycarbonyl isothiocyanate → 1-(3-Methoxycarbonyl-2-thioureido)-2-acetamido-5-benzylthiobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methoxycarbonyl isothiocyanate | HCID 552246 | — |
| Reactant | 1-Acetamido-2-amino-4-benzylthiobenzene | HCID 20371189 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 1-(3-Methoxycarbonyl-2-thioureido)-2-acetamido-5-benzylthiobenzene | HCID 20371150 | — |
Reaction Steps
1.6 G. of 1-acetamido-2-amino-4-benzylthiobenzene is dissolved in 32 ml. acetone and treated with 2.4 g. methoxycarbonylisothiocyanate. The mixture is left overnight at room temperature, then concentrated and the residue triturated with ether. Pure 1-(3-methoxycarbonyl-2-thioureido)-2-acetamido-5-benzylthiobenzene is obtained by recrystallization from methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04072696 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-d9058e4b557b4a9ebe983a4dd1b896fd |
| Source note | uspto-grants-1978_02 |