反应详情

1.4 G. of 1-acetamido-2-nitro-4-methoxymethylthiobenzene is treated on a steam bath for 15 minutes with 3 ml. 5N sodium hydroxide and 6 ml. methanol. The mixture is concentrated, extracted with chloroform and the chloroform extracts dried and stripped yielding 1-amino-2-nitro-4-methoxymethylthiobenzene as a red solid.

1. concentrationThe mixture is concentrated
2. extractionextracted with chloroform
3. dry with materialthe chloroform extracts dried