HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methoxycarbonyl isothiocyanate → HCID 20371121, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methoxycarbonyl isothiocyanate | HCID 552246 | — |
| Reactant | 4-[(Prop-2-yn-1-yl)sulfanyl]benzene-1,2-diamine | HCID 20362841 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 20371121 | HCID 20371121 | — |
Reaction Steps
4 G. of 1,2-diamino-4-propargylthiobenzene in 40 ml. aceton is treated with 10 g. of methoxy carbonyl isothiocyanate. The mixture is left overnight at room temperature, stripped under vacuum and the residue triturated with ether. Recrystallization from methanol gives pure 1,2-bis-(3-methoxycarbonyl-2-thioureido)-4-propargylthio-benzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04072696 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-3c083015a9c1455c91ba00da22505a01 |
| Source note | uspto-grants-1978_02 |