HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methoxycarbonyl isothiocyanate → 1-(3-Methoxycarbonyl-2-thioureido)-5-methylthio-2-nitrobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methoxycarbonyl isothiocyanate | HCID 552246 | — |
| Reactant | 5-(Methylthio)-2-nitroaniline | HCID 10535482 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 1-(3-Methoxycarbonyl-2-thioureido)-5-methylthio-2-nitrobenzene | HCID 20371013 | — |
Reaction Steps
1.5 G. 2-amino-4-methylthio-1-nitrobenzene in 30 ml. acetone is treated with 2.5 g. methoxy carbonyl isothiocyanate. After five days the mixture is stripped under vacuum and the residue triturated with methanol yielding 1-(3-methoxycarbonyl-2-thioureido)-5-methylthio-2-nitrobenzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04072696 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-e2419b17992a4f959a0d94d29c9744de |
| Source note | uspto-grants-1978_02 |