HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → N-{4-[(Methylsulfanyl)methoxy]-2-nitrophenyl}acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Chloromethyl methyl sulfide | HCID 16916 | — |
| Reactant | N-(4-hydroxy-2-nitrophenyl)acetamide | HCID 4024832 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | N-{4-[(Methylsulfanyl)methoxy]-2-nitrophenyl}acetamide | HCID 20362815 | — |
Reaction Steps
3.92 G. of 1 -acetamido-4-hydroxy-2-nitrobenzene, 5.8 g. of chloromethyl methyl sulfide and 8.4 g. anhydrous potassium carbonate are refluxed overnight in acetone with stirring, evaporated to dryness, and water added and the product extracted with dichloromethane to give 1-acetamido4-methylthiomethoxy-2-nitrobenzene as an orange gum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04072696 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-590f8d9c1bee4950b6b3cfd764bf2672 |
| Source note | uspto-grants-1978_02 |