HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methoxycarbonyl isothiocyanate → 1,2-Bis-(3-methoxycarbonyl-2-thioureido)-4-n-butylthiobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methoxycarbonyl isothiocyanate | HCID 552246 | — |
| Reactant | 1,2-Diamino-4-n-butylthiobenzene | HCID 20371059 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 1,2-Bis-(3-methoxycarbonyl-2-thioureido)-4-n-butylthiobenzene | HCID 20371001 | — |
Reaction Steps
1.5 G. of 1,2-diamino-4-n-butylthiobenzene in 30 ml. acetone is treated overnight with 4.5 g. methoxy carbonyl isothiocyanate at room temperature. The solution is concentrated, and the residue triturated with methanol and recrystallized from methanol, yielding 1,2-bis-(3-methoxycarbonyl-2-thioureido)-4-n-butylthiobenzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04072696 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-1fcb6efa55084cf587e8dcbb4d3dc644 |
| Source note | uspto-grants-1978_02 |