HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methoxycarbonyl isothiocyanate → 2-Acetamido-1-(3-methoxycarbonyl-2-thioureido)-5-methoxymethylthiobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methoxycarbonyl isothiocyanate | HCID 552246 | — |
| Reactant | 1-Acetamido-2-amino-4-methoxymethylthiobenzene | HCID 20371210 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 2-Acetamido-1-(3-methoxycarbonyl-2-thioureido)-5-methoxymethylthiobenzene | HCID 20371196 | — |
Reaction Steps
1.0 G. of 1-acetamido-2-amino-4-methoxymethylthiobenzene in 30 ml. acetone is treated overnight with 2 g. methoxy carbonyl isothiocyanate at room temperature. The solution is concentrated and the residue triturated with ether. Recrystallization affords 2-acetamido-1-(3-methoxycarbonyl-2-thioureido)-5-methoxymethylthiobenzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04072696 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-c6ddc46331e1461883701730aa13af85 |
| Source note | uspto-grants-1978_02 |