HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methoxycarbonyl isothiocyanate → 4-Carbamoylthio-1-(3-methoxycarbonyl-2-thioureido)-2-nitrobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methoxycarbonyl isothiocyanate | HCID 552246 | — |
| Reactant | 1-Amino-4-carbamoylthio-2-nitrobenzene | HCID 18949771 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 4-Carbamoylthio-1-(3-methoxycarbonyl-2-thioureido)-2-nitrobenzene | HCID 20371172 | — |
Reaction Steps
1 G. of 1-amino-4-carbamoylthio-2-nitrobenzene in 20 ml. acetone is treated with 3.0 g. methoxy carbonyl isothiocyanate at room temperature for several days. The solution is concentrated and the residue triturated with methanol to afford 4-carbamoylthio-1-(3-methoxycarbonyl-2-thioureido)-2-nitrobenzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04072696 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-04a64dede676417ab16f660662c95e2c |
| Source note | uspto-grants-1978_02 |