Peracetic Acid → HCID 131711029, compound

HRID 616166Notes

Reaction equation

HRID 616166 reaction equation
[CH3:1][NH:2][C:3]([O:5][N:6]=[C:7]1[S:12][CH2:11][S:10](=[O:13])[CH2:9][S:8]1)=[O:4].C(OO)(=[O:16])C>>[CH3:1][NH:2][C:3]([O:5][N:6]=[C:7]1[S:12][CH2:11][S:10](=[O:16])(=[O:13])[CH2:9][S:8]1)=[O:4]

Participants

3

Reactant 2

HCID 6585Peracetic AcidHCID 20371413HCID 20371413, compound

Product 1

HCID 131711029HCID 131711029, compound

Procedure

2-(Methylcarbamoyloximino)-1,3,5-trithiane-5-oxide prepared by the method of Example IV was further reacted with 5 ml of peracetic acid and left standing for 18 hours at room temperature. Concentrating under reduced pressure yielding 0.15g of a solid residue. Crystallization from acetonitrile yielded a solid, m.p. 174°-177° C (decomp.)

Workup

  1. waitleft
  2. concentrationConcentrating under reduced pressure

Sources & evidence

ORD record
ord-e8dd5b5ea163425094a34cab5869c814
Source dataset
uspto-grants-1978_02
Patent number
US04072750

Reaction notes

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