HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aspirin → HCID 10424739, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aspirin | HCID 2244 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-Acetoxybenzoyl chloride | HCID 79668 | — |
| Reactant | 4-Amino-2,6-dichlorophenol | HCID 80037 | — |
| Product | HCID 10424739 | HCID 10424739 | 71.1% |
Reaction Steps
Acetylsalicylic acid chloride prepared from acetylsalicylic acid and thionyl chloride was condensed with 4-amino-2,6-dichlorophenol followed by deacetylation to yield 3',5'-dichloro-2,4'-dihydroxybenzanilide (4 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04072753 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-e6e68c01c6314ee7810acffb27bed9d3 |
| Source note | uspto-grants-1978_02 |