HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20371578, compound → HCID 20434099, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20371578 | HCID 20371578 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 20434099 | HCID 20434099 | — |
Reaction Steps
One g of α-(3,4-dimethoxyphenethylaminomethyl)-2-benzyloxybenzylalcohol hydrochloride, 0.3 g of 10 % palladium-carbon and 30 ml of 80 % aqueous isopropanol are treated in the same manner as described in Example 1-(c). 0.75 g of α-(3,4-dimethoxyphenethylaminomethyl)-2-hydroxybenzylalcohol hydrochloride are obtained. M.p. 141° - 143° C(decomp.) (recrystallized from a mixture of ethanol and ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04072759 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-9a08e394dacb4b41b294f436a7154f34 |
| Source note | uspto-grants-1978_02 |