Methyl iodide → HCID 20369327, compound

HRID 616286Notes

Reaction equation

HRID 616286 reaction equation
[C:1]([NH:4][C:5]1[CH:13]=[CH:12][C:8]([C:9](=[S:11])[NH2:10])=[CH:7][CH:6]=1)(=[O:3])[CH3:2].[CH3:14][I:15]>CC(C)=O>[IH:15].[C:1]([NH:4][C:5]1[CH:13]=[CH:12][C:8]([C:9]([S:11][CH3:14])=[NH:10])=[CH:7][CH:6]=1)(=[O:3])[CH3:2]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 3000565N-(4-carbamothioylphenyl)acetamide

Product 1

HCID 20369327HCID 20369327, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

To a mixture of 2.7 g. (0.014 mole) of p-acetamidobenzthioamide in 100 ml. of acetone is added 2.6 ml. of methyl iodide, and the resulting reaction mixture allowed to stir at room temperature overnight. The intermediate product is filtered and dried, 4.4 g., m.p. 216°-217° C.

Workup

  1. additionTo a mixture of 2.7 g
  2. filtrationThe intermediate product is filtered
  3. customdried

Sources & evidence

ORD record
ord-19a1acc43dbd4075afa84e902d04bc73
Source dataset
uspto-grants-1978_02
Patent number
US04073783

Reaction notes

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